Synthesis of various bisphosphiamindo ligand and their chalcogenide derivatives

Saha, Baidehi and Panda, Tarun K (2018) Synthesis of various bisphosphiamindo ligand and their chalcogenide derivatives. Masters thesis, Indian Institute of Technology, Hyderabad.

[img] Text
Thesis_Msc_CY_3949.pdf - Submitted Version
Restricted to Repository staff only until June 2020.

Download (1MB) | Request a copy


In this report, I have described the synthesis of P-N ligands as ligand 1 [N,N'-(hexane-1,6-diyl)bis(P,P-diphenylphosphinoselenoic amide)] , ligand 2 [N,N'-(hexane-1,6-diyl)bis(P,P-diphenylphosphinothioic amide)], and ligand 3 [N,N'-(hexane-1,6-diyl)bis(P,P-diphenylphosphinic amide)]. The reaction between different amine and PPh2Cl in ratio of 1:2 in toluene solution in presence of Et3N (2 molar) at room temperature for 24 h followed by the addition of elemental S/Se and H2O2 and further keeping for stirring for 12 h afforded these products. All of these compounds are characterized by 1

[error in script]
IITH Creators:
IITH CreatorsORCiD
Panda, Tarun K
Item Type: Thesis (Masters)
Subjects: Chemistry
Divisions: Department of Chemistry
Depositing User: Team Library
Date Deposited: 22 May 2018 11:37
Last Modified: 22 May 2018 11:37
Publisher URL:
Related URLs:

Actions (login required)

View Item View Item
Statistics for RAIITH ePrint 3949 Statistics for this ePrint Item